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[Dedicated to the New National Standard] ST109B1 Intelligent Sulfur Dioxide Analyzer for Food and Pharmaceuticals

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[Dedicated to the New National Standard] ST109B1 Intelligent Sulfur Dioxide Analyzer for Food and Pharmaceuticals

Supported by technological innovation and quality management, with the concept of developing domestically-original instruments and equipment, and adhering to the principle of putting ourselves first, we have developed and manufactured a series of intelligent laboratory instruments and equipment, online atmospheric monitoring equipment, etc. with leading performance and reliable quality.

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◉ Product Introduction

Specialized instruments supporting the new national standard for food sulfur dioxide (sulfur dioxide testing in traditional Chinese medicine using the Chinese Pharmacopoeia method): the ST109A, ST109B1, ST109C, and ST109D series are all equipped as standard with automatic reagent addition and automatic nitrogen blowing control functions (a national first)!!!


R&D Background:


      With the release of the new national standard GB5009.34-2022 Determination of Sulfur Dioxide in Foods, the methods for determining sulfur dioxide in foods and sulfur dioxide in Chinese medicinal materials under the Chinese Pharmacopoeia have become largely consistent. Based on the new national standard and Pharmacopoeia methods, Jinan Shengtai Technology has jointly developed four specialized testing instruments: ST109A, ST109B1, ST109C, and ST109D.


Product Features:

      * Heating method: Automatic far-infrared ceramic heating management system with automatic dry-burn protection technology;

      * Cooling method: Integrated design with a built-in compressor in the main unit, automatically completing internal cooling-water circulation without the need for an external chiller;

      * Condenser design: Reflux condenser specifically designed for national standards;

      * Control system: Automatic temperature-rise technology, with selectable gentle-boiling and full-boiling heating modes; automatic timer: 0-999 min;

      * Reagent addition: Reagents can be added automatically via a high-precision reagent dispensing pump, eliminating manual operation;

      * Nitrogen control: Controlled by a rotameter; range: 100-2000ml/min;


Technical Parameters:

1. Built-in cooling-water circulation unit: The integrated cooling-water circulation system of the main unit shall include a built-in compressor, built-in cooling-water tank, automatic water pump, radiator, fan, and other components. A built-in compressor refrigeration circulation system shall be installed inside the main unit. During operation, the compressor system automatically starts and stops according to the cooling-water temperature, without manual switching. The built-in compressor shall be integrated with the main unit.

2. Short-circuit protection and automatic drying function: Under high-temperature and humid operating conditions, the heating area is highly susceptible to moisture, which may cause circuit short circuits. The main unit shall be designed with leakage protection and an automatic drying function for the heating area. The drying time can be set from 0-999 seconds. When a single heating area is damp and short-circuited, the drying function can be activated to restore the moisture-affected circuit, allowing the equipment to return to normal operating condition.

3. The main unit shall be designed with automatic distillation and automatic stop systems. An over-distillation protection device shall be designed at each distillate outlet. After distillation is completed, the system can automatically lock the distillate outlet, ensuring that the distillation operation is completed automatically and quantitatively.

4. Equipped with multi-level administrator permission settings, enabling storage management and export of experimental data. According to user requirements, it can interface with the lims system to upload experimental operation data.


Comparison of New and Old National Standard Testing Methods for Sulfur Dioxide in Foods (Method I)

GB5009.34-2016 GB5009.34-2022 (New National Standard)
Test MethodTitration MethodThe titration method has been changed to acid-base titration, with Method II spectrophotometry and Method III ion chromatography added.
Testing ScopeThis standard specifies methods for determining total sulfur dioxide in foods such as preserved fruits, dried vegetables, rice flour products, vermicelli, sugar, edible fungi, and wine.The first method is acid-base titration, applicable to the determination of sulfur dioxide in food;
The second method is spectrophotometry. The direct extraction method is applicable to the determination of sulfur dioxide in samples without fat and without color interference in the extract, such as white sugar and white sugar products, starch and starch products, and fresh wet noodle products. The nitrogen-flush distillation extraction method is applicable to the determination of sulfur dioxide in colored samples, such as wine and brown sugar;
The third method is ion chromatography, applicable to the determination of sulfur dioxide in food.
Sample Preparation5g of homogeneous sample (accurate to 0.001g; the sample amount may be determined according to the content level); for liquid samples, directly pipette 5.00mL–10.00mL of sample; add 250ml of water; add 10ml of hydrochloric acid.Take 20 g–100 g of a solid or semi-fluid sample (accurate to 0.01 g; the sample amount may be determined according to the content level); take 20 mL (g)–200 mL (g) of a liquid sample; add 20-500ml of water; add 10ml of 6mol/L hydrochloric acid.
Whether Nitrogen-Flushed Distillation Is UsedNoNitrogen-flushed distillation, flow rate: 1.0-2.0L/min
Absorption Solution25mL lead acetate absorption solution50mL of 3% hydrogen peroxide solution (Method I)
Distillation MethodCollect 200ml of distillate, then continue distillation for 1 minute. Rinse the apparatus inserted into the absorption solution with a small amount of distilled water.Heat the solution in the flask to boiling and maintain slight boiling for 1.5h.
Titration MethodSequentially add 10mL of hydrochloric acid and 1mL of starch indicator solution to the removed iodine flask. After mixing thoroughly, titrate with iodine standard solution until the solution turns blue and does not fade within 30s. Conduct a blank test simultaneously.After cooling the absorption solution, mix thoroughly. Add 3 drops of 2.5 mg/mL methyl red ethanol solution indicator to the absorption solution, titrate with sodium hydroxide standard solution (0.01 mol/L) until yellow and the color does not fade within 20 seconds, and conduct a blank test simultaneously.
Limit of Detection and Limit of QuantificationWhen 5g of a solid sample is taken, the method limit of detection (LOD) is 3.0mg/kg and the limit of quantification is 10.0mg/kg; when 10mL of a liquid sample is taken, the method limit of detection (LOD) is 1.5mg/L and the limit of quantification is 5.0mg/L.When 0.01mol/L sodium hydroxide titrant is used, with a solid or semi-fluid sample weight of 35g, the limit of detection is 1mg/kg and the limit of quantification is 10mg/kg; with a liquid sample volume of 50mL (g), the limit of detection is 1mg/L (mg/kg) and the limit of quantification is 6 mg/L (mg/kg).
Recommended Product ModelsST106-1RW (distillation pretreatment), ST106K2 (fully automatic, directly provides test results.)ST109 full series (A is a six-position fully automatic model that directly provides test results; B is six-position; C is an eight-position cost-effective model; D is a dedicated unit for ion chromatography water-vapor distillation). The entire series is equipped as standard with automatic acid addition and nitrogen control devices (A uses a digital imported nitrogen controller; other models use a rotameter). The entire series is compatible with sulfur dioxide testing in traditional Chinese medicine and Chinese medicinal materials.


◉ Specifications

Comparison Table of Product Parameters for Jinan Shengtai Technology ST109 Series Intelligent Sulfur Dioxide Analyzers
ModelST109AST109BST109CST109D
Applicable StandardsGB5009.34-2022 “Determination of Sulfur Dioxide in Foods”, and the 2015 and 2020 editions of the Chinese Pharmacopoeia for methods of determining sulfur dioxide in traditional Chinese medicine and Chinese medicinal materials;
Corresponding StandardGB5009.34-2022 Method I, Method IIGB5009.34-2022 Method I, Method IIGB5009.34-2022 Method I, Method IIGB5009.34-2022 Method III
Product PositioningHigh-end, fully automaticStandard VersionCost-effective VersionDedicated Unit for Water-Vapor Distillation
Number of Samples6686
Flask CapacityStandard 1000ml two-neck flaskCustomized 1000ml two-neck flaskStandard 1000ml two-neck flaskStandard 500ml two-neck flask
Heating MethodFar-infrared ceramic heatingFar-infrared ceramic heatingFar-infrared ceramic heatingBuilt-in steam source for water-vapor heating
Condenser StructureReflux type, semi-enclosed structureReflux condenserReflux type, semi-enclosed structureSerpentine condenser
Automatic acid additionAutomatic acid additionAutomatic acid additionAutomatic acid additionAutomatic acid addition
Nitrogen ControlDigitally adjustable nitrogen gas distribution systemRotameter (200-2000ml/min)Rotameter (200-2000ml/min)Rotameter (200-2000ml/min)
Cooling MethodExternal cooling water circulatorBuilt-in compressor self-circulating cooling systemExternal cooling water circulatorExternal cooling water circulator
Control MethodDesktop computerLCD touchscreenLCD touchscreenLCD touchscreen
Automatic TitrationHigh-precision syringe pump automatic titrationNoneNone——
Endpoint DetectionHigh-precision visual sensor that fully simulates the human eye and automatically identifies the titration endpointNoneNoneNone
Rated Power3500W3600W4500W3000W
Overall Dimensions (mm)735×650×670960×575×410940×650×680960×500×730


◉ Success Stories

[Dedicated to the New National Standard] ST109B1 Intelligent Sulfur Dioxide Analyzer for Food and Pharmaceuticals

[Dedicated to the New National Standard] ST109B1 Intelligent Sulfur Dioxide Analyzer for Food and Pharmaceuticals

[Dedicated to the New National Standard] ST109B1 Intelligent Sulfur Dioxide Analyzer for Food and Pharmaceuticals

[Dedicated to the New National Standard] ST109B1 Intelligent Sulfur Dioxide Analyzer for Food and Pharmaceuticals

[Dedicated to the New National Standard] ST109B1 Intelligent Sulfur Dioxide Analyzer for Food and Pharmaceuticals

[Dedicated to the New National Standard] ST109B1 Intelligent Sulfur Dioxide Analyzer for Food and Pharmaceuticals

[Dedicated to the New National Standard] ST109B1 Intelligent Sulfur Dioxide Analyzer for Food and Pharmaceuticals

[Dedicated to the New National Standard] ST109B1 Intelligent Sulfur Dioxide Analyzer for Food and Pharmaceuticals

[Dedicated to the New National Standard] ST109B1 Intelligent Sulfur Dioxide Analyzer for Food and Pharmaceuticals

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